{"text_format":"1","workbook":"xlsx","n_sheets":6,"sheets":["Version Information","Overview and Explanations","Attributes","Field Samples","Separation-Processing Samples","Data Validation"],"not_rendered":{"charts":0,"images":6,"macros":1,"external_links":1,"defined_names":30,"comments":2,"pivot_tables":0},"unopened":[],"bounds":{"document_bytes":16777216,"sheet_cells":100000,"rows_first":2000,"rows_last":500,"rows_between":2000,"halvings":0,"cell_chars":16384,"cell_head_chars":4096},"cells_cut":0,"cells_raw":0,"read":"whole","date_system":"1900"}

{"sheet":"Version Information","index":0,"n_rows":13,"n_cols":3,"rows_kept":13,"cut":false,"hidden":false,"merged":[]}
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["Version Number","Notes","Date"]
[1,"Initial version","2020-08-31"]

{"sheet":"Overview and Explanations","index":1,"n_rows":9,"n_cols":6,"rows_kept":9,"cut":false,"hidden":false,"merged":[[7,4,7,5],[8,4,8,5],[0,1,0,5],[6,4,6,5],[5,4,5,5],[2,1,2,3],[2,4,2,5],[1,1,1,5]]}
[null,"Overview"]
[null,"All results recorded in this template will be made publicly available on NETL's database exchange web portal (                                            ).  The focus is to characterize the bulk elemental concentration and mineralogy of rare earth elements in coal and coal by-product material during the initial field sampling in order to provide data needed to determine the best path forward.\n\nThe Attributes tab contains definitions and examples to assist in determining the correct dropdown item(s) to select in both of the Field Samples tabs.  The                  contains step by step information on how to fill out each column within the sample analysis tabs below.  In order to maintain the NETL database's integrity, researcher's should do their best to accurately and precisely describe all information about the samples that is publicly releasable.  Please send all email user questions to                                                    or contact your Federal Project Manager.\n\n \n\n"]
[null,"Coal Basins",null,null,"Researcher Analytical Technique Notes"]
[null,null,null,null,"ICP-MS","Inductively Coupled Plasma Mass Spectrometry"]
[null,null,null,null,"ICP-OES","Inductively Coupled Plasma Optical Emission Spectrometry "]
[null,null,null,null,"EPA methods 6010, 6020, and 7000 were followed for analysis of samples by ICP-MS and ICP-OES"]
[null,null,null,null,"BDL = Below Detection limit"]
[null,null,null,null,"NETL Digestion Procedure for Bulk Elemental Analysis of Solids"]
[null,null,null,null,"There are many digestion procedures that can be employed for inductively coupled plasma mass spectrometry (ICP-MS) or inductively coupled plasma optical emission spectrometry (ICP-OES) analysis (bulk elemental analysis) of solid coal by-products.  One method employed by NETL-RIC is described below.  Note that it is also critical for the lab to determine the percent recoveries of the rare earths and other elements from certified reference materials.  This serves as a check on the digestion procedure, as well as the analytical procedure.  Also note that ICP-OES has inferior detection limits for the rare earths as compared to ICP-MS.\n\n      In the NETL digestion procedure, solid samples were prepared by mixing pulverized sample with calcined LiBO2 (lithium metaborate) at a ratio of 1:8.  Prior to fusion, samples were mixed by stirring with a platinum rod in a 99.95% platinum crucible.  The open crucibles were heated to 1100°C for five minutes in a Phoenix microwave muffle furnace (CEM).  After 5 minutes, the melt was removed from the oven and allowed to cool to a homogeneous glass.  The glass was digested in 5% HNO3 on low heat with stirring.  To ensure that the sample glass was completely digested, the platinum crucibles were rinsed 3x with 5% HNO3 and the sample was diluted to a final volume of 100 ml.  These samples were further diluted in 2% HNO3 before analysis to determine the optimal balance between internal standard recovery and limit of detection.  For solid samples containing significant carbon content, samples were dried and ashed in a Leco Thermogravimetric Analyzer (TGA701) for one hour under nitrogen at 107°C for drying and then for five hours under air at 550°C for ashing. \n\nReference:\n\n\"Analysis of Rare Earth Elements in Geologic Samples using Inductively Coupled Plasma Mass Spectrometry\"\nTracy Bank, Elliot Roth, Phillip Tinker, Evan Granite, DOE Topical Report, available on the"]

{"sheet":"Attributes","index":2,"n_rows":40,"n_cols":6,"rows_kept":40,"cut":false,"hidden":false,"merged":[[15,3,15,5],[17,3,17,5],[16,3,16,5],[18,3,18,5],[19,3,19,5],[20,3,20,5],[21,3,21,5],[22,3,22,5],[33,3,33,5],[34,3,34,5],[39,3,39,5],[27,3,27,5],[28,3,28,5],[29,3,29,5],[30,3,30,5],[31,3,31,5],[32,3,32,5],[37,3,37,5],[24,0,24,2],[36,3,36,5],[35,3,35,5],[23,3,23,5],[38,3,38,5],[24,3,24,5],[26,3,26,5],[25,3,25,5]]}
[null,null,null,"Level 1 Attribute","Level 2 Attribute","Level 3 Attribute"]
[null,null,null,"Resource Production","Coal Reserve","Coal"]
[null,null,null,"Processing","Coal Mining","Clean Coal"]
[null,null,null,"Utilization","Coal Separations","Bottom Ash"]
[null,null,null,null,"Feed  Coal","Fly Ash"]
[null,null,null,null,"Energy Conversion Processes","Ash"]
[null,null,null,null,"Other","Refuse"]
[null,null,null,null,null,"Fine Coal By-Product"]
[null,null,null,null,null,"Coarse Refuse"]
[null,null,null,null,null,"Disposed Combustion By-Products"]
[null,null,null,null,null,"Coal Mine Drainage"]
[null,null,null,null,null,"Acid Mine Drainage"]
[null,null,null,null,null,"Acid Mine Drainage - Sludge"]
[null,null,null,null,null,"Aqueous"]
[null,null,null,null,null,"Other"]
[]
[null,null,null,"Level 1 Attributes: Based on the preparation point of collection, the three level 1 attributes refer to the point of recovery in the coal value process chain on the highest trichotomy level."]
[null,null,null,"Resource Production"]
[null,null,null,"Data in Resource Production reflect characterization of the REEs in resources as they exist in their natural environment, and materials that are produced during mining operations.  These data include core samples, road cuts, outcrops, raw coal grab samples, and aqueous by-products."]
[null,null,null,"Processing"]
[null,null,null,"These data reflect REE characterization results for “as received” or run-of mine material from a number of coal preparation plants, in-plant streams, product streams (refuse, fine coal, and clean coal), and aqueous by-products. "]
[null,null,null,"Utilization"]
[null,null,null,"These data reflect REE characterization results of feed coals as they arrive at the power plant, refuse and coal by-products (fly ash and bottom ash), and aqueous by-products generated at the plant. These materials include grab samples taken at several by-product storage/disposal sites.  Samples can include aqueous effluents from processing facilities, material found in ash ponds, coal mine drainage, and runoff from storage piles."]
[]
["Figure 1. Coal Value Chain Opportunities for REE Recovery.",null,null,"Level 2 Attributes: Based on the preparation point of collection, level 2 attributes refer to more specific points of recovery in the coal value process chain from Resource Production through Processing and Utilization."]
[null,null,null,"Coal Reserve"]
[null,null,null,"Underground and surface coal not yet mined within the United States (e.g., Basin A coal)"]
[null,null,null,"Coal Mining"]
[null,null,null,"Coal that has been extracted from the earth through production processes (e.g., Mine A -  run of mine)"]
[null,null,null,"Coal Separations"]
[null,null,null,"Coal that has undergone washing, dewatering, crushing, and sieving (and or other classifying steps) resulting in clean coal for utilization and by-products such as slurries, refuse, and out-of-spec sized product (e.g.,  Mine A - midlings refuse)"]
[null,null,null,"Feed Coal"]
[null,null,null,"Clean Coal that has been approved for utilization and has been pulverized to plant specs (Power plant A - clean coal pulverized rejects)"]
[null,null,null,"Energy Conversion Processes"]
[null,null,null,"Coal that has been utilized and converted into energy through the power production process (Power Plant A  - Fly Ash)"]
[null,null,null,"Other"]
[null,null,null,"Coal that does not fall into the above categories "]
[]
[null,null,null,"Level 3 Attributes"]
[null,null,null,"Self Evident"]

{"sheet":"Field Samples","index":3,"n_rows":6,"n_cols":130,"rows_kept":6,"cut":false,"hidden":false,"merged":[[4,3,4,4],[4,102,4,118],[0,0,0,7],[3,99,3,118],[4,14,4,17],[4,5,4,13],[3,5,3,17],[4,38,4,76],[4,77,4,80],[4,123,4,124],[3,123,3,128],[4,31,4,34],[4,21,4,25],[4,26,4,30],[4,81,4,94],[3,35,3,98],[3,119,3,122],[4,119,4,122],[4,35,4,37],[4,99,4,101]]}
["Field Site Sampling Material Identification and Characterization"]
[]
[]
[null,null,null,null,null,"Researcher Field Sampling Data Inputs",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"Primary Elemental Identification Technique",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"Secondary Elemental Identification Technique (If Measured)",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"XRD, Phase Identification (If measured)",null,null,null,"SEM-EDX (If measured)"]
[null,null,null,"Sample Reference # for Analyses on Sample Source",null,"Origin of the Sample and Description",null,null,null,null,null,null,null,null,"Location of Sampling Site",null,null,null,null,null,null,"Proximate Analysis (Wt%)",null,null,null,null,"Ultimate Analysis (%)",null,null,null,null,"CHNS Analysis (%)",null,null,null,"Analysis Description/Method",null,null,"Critical Minerals (ppm)",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"Other Elements (ppm)",null,null,null,"Lanthanides (ppm)",null,null,null,null,null,null,null,null,null,null,null,null,null,"Total REE (ppm)","Total REE+Y (ppm)","Total REE +Y + CM (ppm)",null,"Analysis Description Method",null,null,"Results (ppm)"]
["Sample Reference #\n(# required to enable calculations)","Sample Type","Description","Furthest Upstream Sample Ref #","Previous Upstream Sample Ref #","Level 1 Attribute","Level 2 Attribute","Level 3 Attribute","Coal Basin","Geological Group","Associated Coal Bed/Zone/Seam","State","County","Site","State2","County2","Site2","Location2","Size Fraction Analyzed (µm) ","% Moisture, As-Received","%Ash, Dry","Sulfur ","Moisture","Volatile Matter ","Ash","Fixed Carbon","Carbon","Hydrogen","Sulfur","Oxygen ","Nitrogen","Carbon2","H","N","S","Digestion Method","Analytical Technique","Measurement Basis","Al","Sb","As","BaSO4","Be","Bi","Cs","Cr","Co","CaF2","Ga","Ge","Graphite","Hf","He","In","Li","Mg","Mn","Nb","Ru","Rh","Pd","Os","Ir","Pt","Potash","Re","Rb","Sc","Sr","Ta","Te","Sn","Ti","W","U","V","Zr","Y","Other2","Other3","Other4","La\n57","Ce\n58","Pr\n59","Nd\n60","Sm\n62","Eu\n63","Gd\n64","Tb\n65","Dy\n66","Ho\n67","Er\n68","Tm\n69","Yb\n70","Lu\n71","Lanthanides","Lanthanides+Y","Lanthanides + Y + Critical Minerals","Notes","Secondary Analytical Technique","Secondary Digestion Method","Measurement Basis2","  Al3\n13","  Ca4\n20","  Fe5\n26","  K6\n19","  Mg7\n12","  Na8\n11","  P2\n15","  Ti2\n22","SiO2*","Zr\n  402","Sn\n  502","Other6","Other8","Other9","Other10","Other11","Notes3","Major Phases","Minor Phases","Trace Phases ","Notes2","Mineral/particle/crystal","Size","Mineral/particle/crystal2","Size3","Mineral/particle/crystal3","Size4","Notes4"]

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["Separation-Processing Samples"]
[]
[]
[null,null,null,null,null,"Researcher Field Sampling Data Inputs",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"Primary Elemental Identification Technique",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"Secondary Elemental Identification Technique (If Measured)",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"XRD, Phase Identification (If measured)",null,null,null,"SEM-EDX (If measured)"]
[null,null,null,"Sample Reference # for Analyses on Sample Source",null,"Origin of the Sample and Description",null,null,null,null,null,null,null,null,"Location of Sampling Site",null,null,null,null,null,null,"Proximate Analysis (Wt%)",null,null,null,null,"Ultimate Analysis (%)",null,null,null,null,"CHNS Analysis (%)",null,null,null,"Analysis Description/Method",null,null,"Critical Minerals (ppm)",null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,null,"Other Elements (ppm)",null,null,null,"Lanthanides (ppm)",null,null,null,null,null,null,null,null,null,null,null,null,null,"Total REE (ppm)","Total REE+Y (ppm)","Total REE +Y + CM (ppm)",null,"Analysis Description Method",null,null,"Results (ppm)"]
["Sample Reference #\n(# required to enable calculations)","Sample Type","Description","Furthest Upstream Sample Ref #","Previous Upstream Sample Ref #","Level 1 Attribute","Level 2 Attribute","Level 3 Attribute","Coal Basin","Geological Group","Associated Coal Bed/Zone/Seam","State","County","Site","State2","County2","Site2","Location2","Size Fraction Analyzed (µm) ","% Moisture, As-Received","%Ash, Dry","Sulfur ","Moisture","Volatile Matter ","Ash","Fixed Carbon","Carbon","Hydrogen","Sulfur","Oxygen ","Nitrogen","Carbon2","H","N","S","Digestion Method","Analytical Technique","Measurement Basis","Al","Sb","As","BaSO4","Be","Bi","Cs","Cr","Co","CaF2","Ga","Ge","Graphite","Hf","He","In","Li","Mg","Mn","Nb","Ru","Rh","Pd","Os","Ir","Pt","Potash","Re","Rb","Sc","Sr","Ta","Te","Sn","Ti","W","U","V","Zr","Y","Other2","Other3","Other4","La\n57","Ce\n58","Pr\n59","Nd\n60","Sm\n62","Eu\n63","Gd\n64","Tb\n65","Dy\n66","Ho\n67","Er\n68","Tm\n69","Yb\n70","Lu\n71","Lanthanides","Lanthanides+Y","Lanthanides + Y + Critical Minerals","Notes","Secondary Analytical Technique","Secondary Digestion Method","Measurement Basis2","  Al3\n13","  Ca4\n20","  Fe5\n26","  K6\n19","  Mg7\n12","  Na8\n11","  P2\n15","  Ti2\n22","SiO2*","Zr\n  402","Sn\n  502","Other6","Other8","Other9","Other10","Other11","Notes3","Major Phases","Minor Phases","Trace Phases ","Notes2","Mineral/particle/crystal","Size","Mineral/particle/crystal2","Size3","Mineral/particle/crystal3","Size4","Notes4"]
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